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(1) Take raw Rehmannia root and stew it according to the wine stewing method (General Rule 0213) until the wine is absorbed, take it out, dry it in the sun until the mucus on the skin is slightly dry, cut it into thick slices or blocks, and dry it. For every 100kg of raw Rehmannia root, use 30-50kg of yellow wine.
(2) Take raw Rehmannia root and steam it according to the steaming method (General Rule 0213) until it is black and moist, take it out, dry it in the sun until it is about 80% dry, cut it into thick slices or blocks, and dry it.
This product is irregular pieces and fragments of different sizes and thicknesses. The surface is black, shiny, and sticky. It is soft and tough, not easy to break, and the cross section is black and shiny. It has a slight odor and tastes sweet.
Take 1g of the powder of this product, add 50ml of 80% methanol, ultrasonically treat for 30 minutes, filter, evaporate the filtrate, add 5ml of water to dissolve the residue, shake and extract 4 times with water-saturated n-butanol, 10ml each time, combine the n-butanol solution, evaporate to dryness, add 2ml of methanol to dissolve the residue, and use it as the test solution. Take another reference substance of Verbascum saccharum officinale, add methanol to make a solution containing 1mg per 1ml, as the reference solution. According to the thin layer chromatography method (General Rule 0502), take 5μ1 of the test solution and 2μ1 of the reference solution, respectively, and spot them on the same silica gel G thin layer plate, use ethyl acetate-methanol-formic acid (16: 0.5: 2) as the developing agent, develop, take out, dry, soak with 0.1% 2,2-diphenyl-1-naphthyl anhydrous ethanol solution, and dry. In the chromatogram of the test product, the same color spot appears at the corresponding position of the chromatogram of the reference substance.
Same as Rehmannia glutinosa.
Determine according to HPLC (General Rule 0512).
Chromatographic conditions and system suitability test Use octadecylsilane bonded silica gel as filler; methanol-0.1% phosphoric acid solution (5:95) as mobile phase, detection wavelength is 203nm. The theoretical plate number calculated based on Rehmannia glutinosa D peak should not be less than 5000. Preparation of reference solution Take an appropriate amount of Rehmannia glutinosa D reference substance, weigh accurately, add 25% methanol to make a solution containing 70% per 1ml, and obtain.
Preparation of test solution Take this product and cut it into small pieces of about 5mm. After drying under reduced pressure at 80℃ for 24 hours, grind it into coarse powder. Take about 1g, weigh it accurately, put it in a stoppered conical bottle, accurately add 25ml of 25% methanol, weigh it, ultrasonically treat it (power 400W, frequency 50kHz) for 1 hour, let it cool, weigh it again, make up the lost weight with 25% methanol, shake it well, centrifuge it at high speed for 10 minutes, filter the supernatant, and take the filtrate to obtain it. Determination method Accurately take 10% of the reference solution and the test solution respectively, inject them into the liquid chromatograph, and determine them. This product contains not less than 0.050% of Rehmannia glutinosa D (C27 H42O20).
Sweet, slightly warm. It enters the liver and kidney meridians.
Nourishes blood and yin, replenishes essence and fills marrow. Used for blood deficiency, palpitations, irregular menstruation, metrorrhagia, liver and kidney yin deficiency, soreness of waist and knees, bone steaming and hot flashes, night sweats and spermatorrhea, internal heat and thirst, dizziness, tinnitus, and premature graying of hair.
9~15g.
Store in a ventilated and dry place.
Raw Material Selection
Quality Inspection
Processing
Packaging
Quality Control
Storage and Transportation
Raw Material Selection
Chinese Herbal Medicine Cultivation: We strictly select Chinese herbal medicine cultivation bases from authentic medicinal material production areas to ensure the high quality of Chinese medicinal materials.
Herbal Medicine Procurement: We procure high-quality Chinese herbs from around the world to ensure that the herbs are pure, natural, and pollution-free.
Quality Inspection
Raw Material Testing: All purchased Chinese herbs must undergo strict quality inspection before entering the warehouse, including sensory indicators such as appearance, smell, and color, as well as physical and chemical indicators such as component analysis, heavy metal detection, and pesticide residue testing.
Processing
Cleaning: Thoroughly clean the Chinese herbs using clean water sources to remove dirt, impurities, and microorganisms.
Cutting: Based on the characteristics of different Chinese herbs, we adopt appropriate cutting processes, including slicing, segmenting, and shredding, to ensure the efficacy of the herbs and ease of use.
Drying: Use traditional sun-drying and modern drying techniques to ensure that the moisture content of Chinese herbs meets national standards, maintaining the efficacy and storage life of the herbs.
Selection
Screening: Carefully select the Chinese herbs to remove impurities, fragments, and non-conforming items, ensuring the purity and high quality of the herbs.
Sorting: Sort the herbs according to their specifications and grades to ensure product consistency and standardization.
Packaging
Packaging Handling: In a clean packaging workshop, use modern packaging equipment to package the Chinese herbs, ensuring the sealing and hygiene of the packaging and extending the product's shelf life.
Label Identification: Each package is labeled with detailed information, including the name of the herb, specification, place of origin, production date, etc., ensuring the traceability of the product.
Quality Control
Process Monitoring: Strict quality monitoring is carried out at every stage of production to ensure that the products meet national standards and customer requirements.
Final Inspection: Every batch of products undergoes final quality inspection before leaving the factory, including appearance, composition, and microbial indicators, ensuring the safety and efficacy of the products.
Storage and Transportation
Storage: Store the products in warehouses that comply with GSP standards to ensure product quality and stability. Warehouse environment control includes temperature, humidity, and ventilation, ensuring that the herbs do not get damp or deteriorate.
Transportation: Use professional logistics transportation methods to ensure the safety and integrity of the products during transportation, delivering them to customers on time. We cooperate with multiple international logistics companies to ensure fast and efficient global delivery.
Raw Material Selection
Chinese Herbal Medicine Cultivation: We strictly select Chinese herbal medicine cultivation bases from authentic medicinal material production areas to ensure the high quality of Chinese medicinal materials.
Herbal Medicine Procurement: We procure high-quality Chinese herbs from around the world to ensure that the herbs are pure, natural, and pollution-free.
Quality Inspection
Raw Material Testing: All purchased Chinese herbs must undergo strict quality inspection before entering the warehouse, including sensory indicators such as appearance, smell, and color, as well as physical and chemical indicators such as component analysis, heavy metal detection, and pesticide residue testing.
Processing
Cleaning: Thoroughly clean the Chinese herbs using clean water sources to remove dirt, impurities, and microorganisms.
Cutting: Based on the characteristics of different Chinese herbs, we adopt appropriate cutting processes, including slicing, segmenting, and shredding, to ensure the efficacy of the herbs and ease of use.
Drying: Use traditional sun-drying and modern drying techniques to ensure that the moisture content of Chinese herbs meets national standards, maintaining the efficacy and storage life of the herbs.
Selection
Screening: Carefully select the Chinese herbs to remove impurities, fragments, and non-conforming items, ensuring the purity and high quality of the herbs.
Sorting: Sort the herbs according to their specifications and grades to ensure product consistency and standardization.
Packaging
Packaging Handling: In a clean packaging workshop, use modern packaging equipment to package the Chinese herbs, ensuring the sealing and hygiene of the packaging and extending the product's shelf life.
Label Identification: Each package is labeled with detailed information, including the name of the herb, specification, place of origin, production date, etc., ensuring the traceability of the product.
Quality Control
Process Monitoring: Strict quality monitoring is carried out at every stage of production to ensure that the products meet national standards and customer requirements.
Final Inspection: Every batch of products undergoes final quality inspection before leaving the factory, including appearance, composition, and microbial indicators, ensuring the safety and efficacy of the products.
Storage and Transportation
Storage: Store the products in warehouses that comply with GSP standards to ensure product quality and stability. Warehouse environment control includes temperature, humidity, and ventilation, ensuring that the herbs do not get damp or deteriorate.
Transportation: Use professional logistics transportation methods to ensure the safety and integrity of the products during transportation, delivering them to customers on time. We cooperate with multiple international logistics companies to ensure fast and efficient global delivery.
Processing
Cleaning: Thoroughly clean the Chinese herbs using clean water sources to remove dirt, impurities, and microorganisms.
Cutting: Based on the characteristics of different Chinese herbs, we adopt appropriate cutting processes, including slicing, segmenting, and shredding, to ensure the efficacy of the herbs and ease of use.
Drying: Use traditional sun-drying and modern drying techniques to ensure that the moisture content of Chinese herbs meets national standards, maintaining the efficacy and storage life of the herbs.
Selection
Screening: Carefully select the Chinese herbs to remove impurities, fragments, and non-conforming items, ensuring the purity and high quality of the herbs.
Sorting: Sort the herbs according to their specifications and grades to ensure product consistency and standardization.
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